2-Nitrotoluene → alpha-Bromo-2-nitrotoluene

HRID 1927534Notes

Reaction equation

HRID 1927534 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[N+:8]([O-:10])=[O:9].[Br:11]N1C(=O)CCC1=O>>[Br:11][CH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[N+:8]([O-:10])=[O:9]

Participants

3

Reactant 2

HCID 69442-NitrotolueneHCID 67184N-bromobutanimide

Product 1

HCID 77569alpha-Bromo-2-nitrotoluene

Procedure

1-Methyl-2-nitro-benzene was reacted with N-bromosuccinimide as described in the synthesis of Example 1e to obtain the title compound.

Workup

  1. customas described in the synthesis of Example 1e

Sources & evidence

ORD record
ord-53df094f0e714b41a57eba17fd25cdb6
Source dataset
uspto-grants-2012_05
Patent number
US08183234B2

Reaction notes

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