alpha-Bromo-2-nitrotoluene → HCID 68427056, compound

Participants

Reaction Steps

4-Bromo-3-mercapto-benzoic acid methyl ester was reacted with 1-bromomethyl-2-nitro-benzene as described in the synthesis of Example 1f to obtain the title compound. Yield: (64%); 1H NMR (CDCl3): δ 3.90 (s, 3H, OCH3), 4.55 (s, 2H, CH2), 7.40-7.55 (m, 3H, Ar), 7.60 (d, 1H, Ar), 7.70 (d, 1H, Ar), 7.90 (d, 1H, Ar), 8.10 (d, 1H, Ar).

Provenance & Evidence