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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1927544Generated: November 3, 2026

2-Cyclohexen-1-one, 4,4-dimethyl- → Cyclohexanone, 4,4-dimethyl-

https://huagongshe.com/reaction/1927544

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-Cyclohexen-1-one, 4,4-dimethyl-HCID 136839—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventPentaneHCID 8003—
ProductCyclohexanone, 4,4-dimethyl-HCID 13816698.3%

Reaction Steps

4,4-dimethyl-cyclohexen-1-one (5 g, 40.3 mmol) were placed in a hydrogen reaction vessel and n-pentane (15 ml) was added, and Pd/C (500 mg) was added thereto. The hydrogen reaction vessel was pressurized with hydrogen (25 psi), and the reaction was conducted for 30 minutes. After completing the reaction, the solid like material was filtered through Celite and the filtrate was concentrated in vacuo to give the title compound (5 g, 98%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08183243B2
Source datasetuspto-grants-2012_05
ORD IDord-28e3516305bc43158d1b3ad318d497e2
Source noteuspto-grants-2012_05