HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 178442446, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | HCID 178442448 | HCID 178442448 | — |
| Product | HCID 178442446 | HCID 178442446 | — |
Reaction Steps
3-[4-(2,2-dimethylbutyl)-1H-imidazol-2-yl]propanoyl chloride in methylene chloride (0.3 M) (7.8 mL, 2.3 mmol) was added to a rapidly stirred solution of concentrated aqueous ammonium hydroxide (2.5 mL) at 0° C. After stirring at rt for 1 h, the volatiles were removed to afford the title compound, which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183275B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-10479eb569194d9fa7f4d845742d72e0 |
| Source note | uspto-grants-2012_05 |