HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Bromophenyl)boronic acid → 2-(3-Bromo-phenyl)-4-(4-chloro-phenyl)-6-methylpyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Bromophenyl)boronic acid | HCID 2734318 | — |
| Reactant | 4-(4-Chloro-phenyl)-2-iodo-6-methyl-pyridine | HCID 57468642 | — |
| Product | 2-(3-Bromo-phenyl)-4-(4-chloro-phenyl)-6-methylpyridine | HCID 57468750 | — |
Reaction Steps
The title compound was prepared from 4-(4-chloro-phenyl)-2-iodo-6-methyl-pyridine (example A.29) (1.5 g, 5 mmol) and commercially available 3-bromo-benzene-boronic acid (1.005 g, 5 mmol) according to the general procedure IVb. Obtained as a white solid (0.15 g, 8.4%). MS (ISP) 358.0 [(M+H)+], 360.0 [(M+2+H)+] and 362.2 [(M+4+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183262B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-707e40d730e544d886a497d315ae4704 |
| Source note | uspto-grants-2012_05 |