HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4-methyl-6-(4-trifluoromethyl-phenyl)-pyrimidine → HCID 57468778, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4-methyl-6-(4-trifluoromethyl-phenyl)-pyrimidine | HCID 57468614 | — |
| Reactant | HCID 178432450 | HCID 178432450 | — |
| Product | HCID 57468778 | HCID 57468778 | — |
Reaction Steps
The title compound was prepared from 2-chloro-4-methyl-6-(4-trifluoromethyl-phenyl)-pyrimidine (example A.12) (0.4 g, 1.47 mmol) and commercially available 4-bromo-2-methyl-imidazole (0.35 g, 2.17 mmol) according to the general procedure IVa. Obtained as a light brown solid (0.41 g, 70%). MS (ISP) 399.0 [(M+H)+]; mp 180° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183262B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-e89c697c0cac4df1b084d06a48524864 |
| Source note | uspto-grants-2012_05 |