HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57468665, compound → HCID 57468786, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57468665 | HCID 57468665 | — |
| Reactant | HCID 178506559 | HCID 178506559 | — |
| Product | HCID 57468786 | HCID 57468786 | — |
Reaction Steps
The title compound was prepared from 2-chloro-4-(3-chloro-phenyl)-6-trifluoromethyl-pyrimidine (example A.44) (3.12 g, 10.6 mmol) and commercially available 4-iodo-imidazole (2.27 g, 11.7 mmol) according to the general procedure IVa. Obtained as an off-white solid (4.0 g, 83%). MS (ISP) 451.0 [(M+H)+]; mp 202° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183262B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-00a2e76033e94e8b8299cf1953d0b664 |
| Source note | uspto-grants-2012_05 |