HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Iodo-4-methyl-6-(4-trifluoromethyl-phenyl)pyridine → HCID 86615445, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Iodo-4-methyl-6-(4-trifluoromethyl-phenyl)pyridine | HCID 57468682 | — |
| Reactant | HCID 68828138 | HCID 68828138 | — |
| Product | HCID 86615445 | HCID 86615445 | — |
Reaction Steps
The title compound was prepared from 2-iodo-4-methyl-6-(4-trifluoromethyl-phenyl)-pyridine (example A.58) (5.45 g, 15 mmol) and commercially available 2-chloropyridine boronic acid (2.48 g, 15.75 mmol) according to the general procedure IVb. Obtained as an off-white solid (3.82 g, 73%). MS (ISP) 349.2 [(M+H)+] and 351 [(M+2+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183262B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-41ef4dbe8e89416f9dcefa4d9d39f9c7 |
| Source note | uspto-grants-2012_05 |