HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Sulfamoylbenzoic acid → HCID 57468850, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Sulfamoylbenzoic acid | HCID 229352 | — |
| Reactant | HCID 178513396 | HCID 178513396 | — |
| Product | HCID 57468850 | HCID 57468850 | — |
Reaction Steps
The title compound was prepared from N-hydroxy-4-trifluoromethyl-6-(4-trifluoromethyl-phenyl)-pyrimidine-2-carboxamidine (example C.2) (0.176 g, 0.5 mmol) and commercially available 3-sulfamoyl-benzoic acid (0.1 g, 0.5 mmol) according to the general procedure V. Obtained as an off-white solid (0.11 g, 42%). MS (ISN) 514.1 [(M−H)−]; mp 205° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183262B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-90ee9b7164794db291b7538fb1e00914 |
| Source note | uspto-grants-2012_05 |