HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Aminonicotinic acid → HCID 60209354, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Aminonicotinic acid | HCID 18496 | — |
| Reactant | HCID 178513396 | HCID 178513396 | — |
| Product | HCID 60209354 | HCID 60209354 | — |
Reaction Steps
The title compound was prepared from N-hydroxy-4-trifluoromethyl-6-(4-trifluoromethyl-phenyl)-pyrimidine-2-carboxamidine (example C.2) (0.176 g, 0.5 mmol) and commercially available 6-amino-nicotinic acid (0.07 g, 0.5 mmol) according to the general procedure V. Obtained as an off-white solid (0.055 g, 24%). MS (ISP) 453.1 [(M+H)+]; mp 205° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183262B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-c97d044b78f74d47b2dbb462b316f689 |
| Source note | uspto-grants-2012_05 |