HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Pyridinylboronic acid → HCID 68692507, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Pyridinylboronic acid | HCID 2734378 | — |
| Reactant | HCID 57468729 | HCID 57468729 | — |
| Product | HCID 68692507 | HCID 68692507 | — |
Reaction Steps
The title compound was prepared from 4-(4-chloro-phenyl)-2-(2-chloro-pyridin-4-yl)-6-trifluoromethyl-pyrimidine (example E.5) (0.185 g, 0.5 mmol) and commercially available 3-pyridineboronic acid (0.08 g, 0.65 mmol) according to the general procedure VI. Obtained as a white solid (0.018 g, 9%). MS (ISP) 413.1 [(M+H)+]; mp 226° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183262B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-b0f0133197f14bfcbc26dd83eb1ab8cf |
| Source note | uspto-grants-2012_05 |