HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-hydroxy-4-sulfamoylbenzene-1-carboximidamide → HCID 57468870, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-hydroxy-4-sulfamoylbenzene-1-carboximidamide | HCID 612025 | — |
| Reactant | HCID 57468716 | HCID 57468716 | — |
| Product | HCID 57468870 | HCID 57468870 | — |
Reaction Steps
The title compound was prepared from N-hydroxy-4-sulfamoyl-benzamidine [CAS-No. 4476-10-2] (0.16 g, 0.75 mmol) and 4-(3-ethoxy-4-trifluoromethyl-phenyl)-6-trifluoromethyl-pyrimidine-2-carboxylic acid (example D.4) (0.19 g, 0.5 mmol) according to the general procedure V. Obtained as a light yellow solid (0.114 g, 41%). MS (ISP) 560.2 [(M+H)+]; mp 250.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183262B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-f1cfcd748d284d989e051f78175959e9 |
| Source note | uspto-grants-2012_05 |