HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4-trifluoromethyl-6-(4-trifluoromethylphenyl)-pyrimidine → HCID 57468881, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4-trifluoromethyl-6-(4-trifluoromethylphenyl)-pyrimidine | HCID 57468599 | — |
| Reactant | HCID 178420001 | HCID 178420001 | — |
| Product | HCID 57468881 | HCID 57468881 | — |
Reaction Steps
The title compound was prepared from 2-chloro-4-trifluoromethyl-6-(4-trifluoromethyl-phenyl)-pyrimidine (example A.2) (0.16 g, 0.5 mmol) and 4-(1H-[1,2,4]-triazol-3-yl)-pyridine [CAS-No. 14803-99-7] (0.075 g, 0.51 mmol) according to the general procedure IVa. Obtained as a white solid (0.096 g, 44%). MS (ISP) 437.3 [(M+H)+]; mp 248° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183262B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-7407ed9a8f414550870a0f1a5bbf3548 |
| Source note | uspto-grants-2012_05 |