HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Aminosulphonyl)benzeneboronic acid → HCID 57469004, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Aminosulphonyl)benzeneboronic acid | HCID 44119323 | — |
| Reactant | 2-(3-Bromo-phenyl)-6-methyl-4-(4-trifluoromethyl-phenyl)-pyridine | HCID 57468745 | — |
| Product | HCID 57469004 | HCID 57469004 | — |
Reaction Steps
The title compound was prepared from 2-(3-bromo-phenyl)-6-methyl-4-(4-trifluoromethyl-phenyl)-pyridine (example E.21) (0.200 g, 0.51 mmol) and 3-sulfamoyl-benzeneboronic acid (example F.2) (0.102 g, 0.51 mmol) according to the general procedure VI. Obtained as a white solid (0.120 g, 50%). MS (ISP) 467.1 [(M+H)+]; mp 196° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183262B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-189f4247f3d548a784502b61c423e78f |
| Source note | uspto-grants-2012_05 |