HuagongsheHuagongshe Chemistry Print Report · For research reference only
(5-Sulfamoylpyridin-3-yl)boronic acid → HCID 57469012, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (5-Sulfamoylpyridin-3-yl)boronic acid | HCID 57415702 | — |
| Reactant | 2-(3-Bromo-phenyl)-6-methyl-4-(4-trifluoromethyl-phenyl)-pyridine | HCID 57468745 | — |
| Product | HCID 57469012 | HCID 57469012 | — |
Reaction Steps
The title compound was prepared from 2-(3-bromo-phenyl)-6-methyl-4-(4-trifluoromethyl-phenyl)-pyridine (example E.21) (0.200 g, 0.51 mmol) and 3-sulfamoyl-pyridine-5-boronic acid (example F.3) (0.103 g, 0.51 mmol) according to the general procedure VI. Obtained as a white solid (0.015 g, 6%). MS (ISP) 470.3 [(M+H)+]; mp>250° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183262B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-377a4bfd975a4cb68d4a25bc9e1f5587 |
| Source note | uspto-grants-2012_05 |