HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dibromo-1,3-thiazole → HCID 57469013, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dibromo-1,3-thiazole | HCID 2763297 | — |
| Reactant | 2-Iodo-6-methyl-4-(4-trifluoromethyl-phenyl)pyridine | HCID 57468645 | — |
| Product | HCID 57469013 | HCID 57469013 | — |
Reaction Steps
The title compound was prepared from 2-iodo-6-methyl-4-(4-trifluoromethyl-phenyl)-pyridine (example A.31) (4.0 g, 9.36 mmol) and commercially available 2,4-dibromothiazole (2.53 g, 10.4 mmol) according to the general procedure IVc protocol b. Obtained as a side product as a light yellow solid (0.065 g, 2%). MS (ISP) 321.2 [(M+H)+]; mp 103° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183262B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-2d44a1ee9c234904b89a1cf6507441d8 |
| Source note | uspto-grants-2012_05 |