HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57468838, compound → HCID 60209460, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57468838 | HCID 57468838 | — |
| Reactant | 3-[6-Methyl-4-(4-trifluoromethyl-phenyl)pyridin-2-yl]-benzeneboronic acid | HCID 60209341 | — |
| Product | HCID 60209460 | HCID 60209460 | — |
Reaction Steps
The title compound was prepared from 3-[6-methyl-4-(4-trifluoromethyl-phenyl)-pyridin-2-yl]-benzeneboronic acid (example G.9) (0.20 g, 0.56 mmol) and 3-bromo-N-methoxy-benzenesulfonamide (example H.3) (0.149 g, 0.56 mmol) according to the general procedure VI. Obtained as a white solid (0.120 g, 43%). MS (ISP) 499.2 [(M+H)+]; mp 181° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183262B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-22e7569fad68499db501a02c6413288f |
| Source note | uspto-grants-2012_05 |