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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1928301Generated: October 31, 2026

HCID 57468804, compound → HCID 60209465, compound

https://huagongshe.com/reaction/1928301

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 57468804HCID 57468804—
ReactantN-tert-butyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)thiophene-2-sulfonamideHCID 57468817—
ProductHCID 60209465HCID 60209465—

Reaction Steps

The title compound was prepared from 2-(3-bromo-phenyl)-4-methyl-6-(4-trifluoromethyl-phenyl)-pyridine (example E.90) (0.392 g, 1.0 mmol) and N-tert-butyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-thiophene-2-sulfonamide (example F.1) (0.380 g, 1.1 mmol) according to the general procedure VI. Obtained as a white solid (0.409 g, 77%). MS (ISP) 531.3 [(M+H)+]; mp 156° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08183262B2
Source datasetuspto-grants-2012_05
ORD IDord-16021e4d7cbb4f998cf7e8fdecbd30a3
Source noteuspto-grants-2012_05