HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(tert-Butylaminosulphonyl)benzeneboronic acid → HCID 57469036, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(tert-Butylaminosulphonyl)benzeneboronic acid | HCID 44119538 | — |
| Reactant | HCID 57468807 | HCID 57468807 | — |
| Product | HCID 57469036 | HCID 57469036 | — |
Reaction Steps
The title compound was prepared from 2-(4-chloro-phenyl)-6-(4-iodo-imidazol-1-yl)-4-methyl-pyridine (example E.95) (0.198 g, 0.5 mmol) and commercially available 3-(tert-butylsulfamoyl)-benzeneboronic acid (0.141 g, 0.55 mmol) according to the general procedure VI. Obtained as a white solid (0.028 g, 12%). MS (ISP) 482.4 [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183262B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-4e11379c4b834e4089c59e8306b23749 |
| Source note | uspto-grants-2012_05 |