Dimethylsulphamoyl chloride → HCID 68633818, compound

HRID 1928766Notes

Reaction equation

[CH3:1][N:2]([CH3:7])[S:3](Cl)(=[O:5])=[O:4].[O:8]1[C:12]2[CH:13]=[CH:14][CH:15]=[CH:16][C:11]=2[CH:10]([NH:17][C:18]2[CH:27]=[CH:26][C:25]3[C:20](=[CH:21][CH:22]=[C:23]([NH2:28])[CH:24]=3)[N:19]=2)[CH2:9]1>>[O:8]1[C:12]2[CH:13]=[CH:14][CH:15]=[CH:16][C:11]=2[CH:10]([NH:17][C:18]2[CH:27]=[CH:26][C:25]3[C:20](=[CH:21][CH:22]=[C:23]([NH:28][S:3]([N:2]([CH3:7])[CH3:1])(=[O:5])=[O:4])[CH:24]=3)[N:19]=2)[CH2:9]1

Participants

Reactant 2

HCID 83372Dimethylsulphamoyl chloride

HCID 64231785HCID 64231785, compound

Product 1

HCID 68633818HCID 68633818, compound

Procedure

The title compound was prepared in accordance with the general method described in example 66 from dimethylsulfamoylchloride and rac-N2-(2,3-dihydro-benzofuran-3-yl)-quinoline-2,6-diamine; MS: m/e=385.6 (M+H+).

Sources & evidence

ORD record: ord-8d93556f02f14ea59940bf462f86a4c9
Source dataset: uspto-grants-2012_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08183380B2

Reaction notes

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