HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphosgene → HCID 44218424, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphosgene | HCID 94429 | — |
| Reactant | 1-Tert-butylpiperazine | HCID 3530572 | — |
| Reactant | (R)-N2-Indan-1-yl-quinoline-2,6-diamine | HCID 57860958 | — |
| Product | HCID 44218424 | HCID 44218424 | — |
Reaction Steps
The title compound was prepared in accordance with the general method 4 described in example 16 from bis(trichloromethyl) carbonate (44 mg, 0.16 mmol), commercially available N-tert-butylpiperazine (52 mg, 0.363 mmol) and (R)—N2-indan-1-yl-quinoline-2,6-diamine (100 mg, 0.363 mmol); obtained as a white solid (150 mg, 93%); MS: m/e=444.5 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183380B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-ac123ef85308405fb13d07fe6a27f878 |
| Source note | uspto-grants-2012_05 |