Dimethylsulphamoyl chloride → HCID 68640043, compound

HRID 1928826Notes

Reaction equation

[CH3:1][N:2]([CH3:7])[S:3](Cl)(=[O:5])=[O:4].[CH3:8][O:9][C:10]1[CH:11]=[C:12]([CH3:31])[CH:13]=[C:14]2[C:18]=1[CH:17]([NH:19][C:20]1[CH:29]=[CH:28][C:27]3[C:22](=[CH:23][CH:24]=[C:25]([NH2:30])[CH:26]=3)[N:21]=1)[CH2:16][CH2:15]2>>[CH3:8][O:9][C:10]1[CH:11]=[C:12]([CH3:31])[CH:13]=[C:14]2[C:18]=1[CH:17]([NH:19][C:20]1[CH:29]=[CH:28][C:27]3[C:22](=[CH:23][CH:24]=[C:25]([NH:30][S:3]([N:2]([CH3:7])[CH3:1])(=[O:5])=[O:4])[CH:26]=3)[N:21]=1)[CH2:16][CH2:15]2

Participants

Reactant 2

HCID 83372Dimethylsulphamoyl chloride

HCID 68915305HCID 68915305, compound

Product 1

HCID 68640043HCID 68640043, compound

Procedure

The title compound was prepared in accordance with the general method described in example 66 from dimethylsulfamoylchloride and rac-N2-(7-methoxy-5-methyl-indan-1-yl)-quinoline-2,6-diamine; MS: m/e=427.6 (M+H+).

Sources & evidence

ORD record: ord-33393b852e0a4f679c2dc5e940d17be6
Source dataset: uspto-grants-2012_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08183380B2

Reaction notes

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