HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methyl-1-pentanol → 4-(4-methyl-pentyloxy)-1H-indole-2-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methyl-1-pentanol | HCID 12296 | — |
| Reactant | 4-(2,2-Dimethyl-propoxy)-1H-indole-2-carboxylic acid | HCID 66841536 | — |
| Product | 4-(4-methyl-pentyloxy)-1H-indole-2-carboxylic acid | HCID 66842030 | — |
Reaction Steps
This compound is synthesized analogously to (85) from 4-methyl-pentan-1-ol. Yield: 0.61 g (94%). MS (ESI): 260 [M−H]−, 1H-NMR (DMSO-d6): δ (ppm) 12.8 (s, 1H), 11.65 (s, 1H), 7.1 (dd, 1H), 7.0 (s, 1H), 6.98 (d, 1H), 6.48 (d, 1H), 4.05 (t, 2H), 1.77 (t, 2H), 1.63 (m, 1H), 1.35 (m, 2H), 0.9 (d, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183366B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-9a70a878a70a40b2bc1abb63d62bd08d |
| Source note | uspto-grants-2012_05 |