HuagongsheHuagongshe Chemistry Print Report · For research reference only
Selenium Dioxide → HCID 82410987, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Selenium Dioxide | HCID 24007 | — |
| Reactant | HCID 66842179 | HCID 66842179 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 82410987 | HCID 82410987 | — |
Reaction Steps
To a solution of 4-methoxy-3-methyl-benzofuran (J. Chem. Res. Synopses (1996),132) (4 g, 24.66 mmol) in 40 ml of dioxane is added selenium dioxide (3.39 g, 29.59 mmol) and the mixture is heated under reflux for 24 hours. It is then cooled and filtered. The solvent is evaporated and the crude red solid is used as such in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183366B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-f2a519270020424c9fafc0df0295aac9 |
| Source note | uspto-grants-2012_05 |