HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylbenzaldehyde → 3-(p-Methylphenyl)propanal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylbenzaldehyde | HCID 7725 | — |
| Reactant | 4-Methyl cyclohexanepropanal | HCID 58262517 | — |
| Product | 3-(p-Methylphenyl)propanal | HCID 64812 | — |
Reaction Steps
4-Methyl cyclohexanepropanal was similarly prepared as described in Examples I and II. First, 4-methyl benzaldehyde (140 g, commercially available from Mitsubishi Gas Chemical America, Inc.) was used to obtain 3-(4-methyl-phenyl)-propionaldehyde (130 g) with a boiling point of 120° C. at a pressure of 21 mmHg 3-(4-Methyl-phenyl)-propionaldehyde (180 g) was consequently used to provide 4-methyl cyclohexanepropanal (104 g) with a boiling point of 112° C. at a pressure of 24 mmHg
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188023B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-8161592e23ed4177b2470fc2684c2046 |
| Source note | uspto-grants-2012_05 |