4-Chloro-3-nitrobenzenesulfonamide → HCID 57474991, compound

HRID 1929407Notes

Reaction equation

HRID 1929407 reaction equation
[CH2:1]([NH:8][CH2:9][CH2:10][C:11]([O:13][CH2:14][CH3:15])=[O:12])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Cl[C:17]1[CH:22]=[CH:21][C:20](S(N)(=O)=O)=[CH:19][C:18]=1[N+]([O-])=O>>[CH2:14]([O:13][C:11](=[O:12])[CH2:10][CH2:9][N:8]([C:11](=[O:12])[CH2:10][C:22]12[CH2:21][CH:20]3[CH2:1][CH:2]([CH2:7][CH:18]([CH2:19]3)[CH2:17]1)[CH2:3]2)[CH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1)[CH3:15]

Participants

3

Reactant 2

HCID 73244-Chloro-3-nitrobenzenesulfonamideHCID 90196N-(Phenylmethyl)-beta-alanine ethyl ester

Product 1

HCID 57474991HCID 57474991, compound

Procedure

The title compound was prepared by substituting 1-adamantaneacetic acid for EXAMPLE 1A and ethyl 3-(benzylamino)propanoate for 4-chloro-3-nitrobenzenesulfonamide in EXAMPLE 1B.

Sources & evidence

ORD record
ord-2e36b4f897384d63a178a1a31d5a4556
Source dataset
uspto-grants-2012_05
Patent number
US08188077B2

Reaction notes

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