HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 66931525, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Potassium Cyanide | HCID 9032 | — |
| Reactant | Ammonium Carbonate | HCID 517111 | — |
| Reactant | 1-(5-Bromo-2-fluorophenyl)ethanone | HCID 22607476 | — |
| Product | HCID 66931525 | HCID 66931525 | — |
Reaction Steps
The reaction of 1-(5-bromo-2-fluoro-phenyl)-ethanone with potassium cyanide and ammonium carbonate in ethanol in an autoclave at 120° C. for 16 h yielded the title compound as light yellow solid. Mass (calculated) C10H8BrFN2O2 [287.087]; (found) [M−H]−=285, [M+2-H]−=287.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188079B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-de2fdaf7a07a432fb3253cb9937d5414 |
| Source note | uspto-grants-2012_05 |