Ammonia → HCID 24205687, compound

Participants

Reaction Steps

General procedure e from 10 (100%); white needles; mp 198-200° C.; 1H NMR (400.13 MHz) δ 8.06 (d, J=4 Hz, 1H), 7.79 (d, J=2 Hz, 1H), 7.75 (s, 1H), 7.48 (s, 1H), 7.40 (d, J=4 Hz, 2H), 7.30 (t, J=4 Hz, 2H), 7.23 (m, 1H), 7.16 (dd, J=4 Hz, 2 Hz, 1H), 7.09 (s, 1H), 6.00 (s, 2H), 5.15 (s, 2H), 3.23 (m, 2H), 2.23 (t, J=6 Hz, 2H), 1.58 (m, 4H), 1.36 (m, 2H); MS (DCI/NH3) m/e: 486 (M+H)+.

Provenance & Evidence