Ammonia → HCID 24205686, compound

Participants

Reaction Steps

N-(2,3-Methylenedioxy-6-benzyloxy-phenanthr-9-ylmethyl)-5-aminohexanol (13) General procedure f from 10 (95%); white powder; mp 175-177° C.; 1H NMR (400.13 MHz) δ 7.90 (d, J=4 Hz, 1H), 7.86 (d, J=2 Hz, 1H), 7.76 (s, 1H), 7.45 (s, 1H), 7.44 (d, J=4 Hz, 2H), 7.32 (t, J=4 Hz, 2H), 7.26 (m, 1H), 7.24 (dd, J=4 Hz, 2 Hz, 1H), 7.14 (s, 1H), 6.03 (s, 2H), 5.22 (s, 2H), 4.24 (s, 2H), 3.53 (t, J=6 Hz, 2H), 2.72 (t, J=6 Hz, 2H), 1.58 (m, 2H), 1.47 (m, 2H), 1.29 (m, 4H); MS (DCI/NH3) m/e: 458 (M+H)+. Anal. (C29H31O4N) C, H, N.

Provenance & Evidence