HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyethanol → HCID 24857250, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyethanol | HCID 8019 | — |
| Reactant | 4-Chlorophenylboronic acid | HCID 74299 | — |
| Reactant | (2S)-2-Amino-3,3-dimethyl-1-butanol | HCID 2734079 | — |
| Reactant | Methyl 5-bromo-6-hydroxynicotinate | HCID 2764315 | — |
| Product | HCID 24857250 | HCID 24857250 | — |
Reaction Steps
The title compound was synthesized in analogy to the procedure described for the preparation of Example 6, using 5-bromo-1,6-dihydro-6-oxo-3-pyridinecarboxylic acid methyl ester, 2-methoxy-ethanol (commercially available), 4-chlorophenyl-boronic acid (commercially available) and L-tert-leucinol (commercially available) as starting materials. MS (ISP): 407.4 (MH−).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188093B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-f9b3cb1be065485dbad21725f7503ed8 |
| Source note | uspto-grants-2012_05 |