HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxy-1-propanol → HCID 67505185, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxy-1-propanol | HCID 74116 | — |
| Reactant | 5-Bromo-6-chloropyridine-3-carboxylic acid | HCID 285433 | — |
| Reactant | 4-Fluorophenylboronic acid | HCID 285645 | — |
| Reactant | (1R,2R)-2-Aminocyclohexanol | HCID 735777 | — |
| Product | HCID 67505185 | HCID 67505185 | — |
Reaction Steps
The title compound was synthesized in analogy to the procedure described for the preparation of Example 31, using 5-bromo-6-chloro-3-pyridinecarboxylic acid, 3-methoxy-1-propanol (commercially available), 4-fluorophenyl-boronic acid (commercially available), and (1R,2R)-2-amino-cyclohexanol (commercially available) to give the title compound as a colorless solid, MS (ISP): 403.5 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188093B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-28073c83b4774c68b4060bd123a3e379 |
| Source note | uspto-grants-2012_05 |