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HRID1930715

反应详情

EQUATION

反应方程式

HRID 1930715 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)N1CCC(=O)CC1
HCID735900

1-Boc-4-piperidone

C10H17NO3

结构：Cc1cc(C)n(C(C)C(=O)Cl)n1
HCID59333819

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(C)n(C(C)C(=O)C2CN(C(=O)OC(C)(C)C)CCC2=O)n1
HCID59333803

未命名化合物

收率 23.9%

PROCEDURE

实验过程

tert-Butyl 3-(2-(3,5-dimethyl-1H-pyrazol-1-yl)propanoyl)-4-oxopiperidine-1-carboxylate (0.248 g, 23.87% yield) was synthesised from 2-(3,5-dimethyl-1H-pyrazol-1-yl)propanoyl chloride (0.5 g, 2.97 mmol, example 104b) and tert-butyl 4-oxopiperidine-1-carboxylate (1.185 g, 5.95 mmo) by the general procedure for the preparation of diketones.