HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2-(Cyclopentyloxy)acetyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | (Cyclopentyloxy)acetic acid | HCID 13355021 | — |
| Product | 2-(Cyclopentyloxy)acetyl chloride | HCID 86641917 | 100% |
Reaction Steps
2-(Cyclopentyloxy)acetic acid (476mg, 3.3 mmol) was heated to reflux in thionyl chloride (0.365 ml, 5.00 mmol). After 30 min the excess of thionyl chloride was evaporated to afford (2-(cyclopentyloxy)acetyl chloride (3.3 mmol) that was used directly in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188101B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-cba6a54ec743409aa8f5010466e38fb3 |
| Source note | uspto-grants-2012_05 |