Dichloromethane → HCID 178465511, compound

Participants

Reaction Steps

A mixture containing 4-{4-[2-(phenoxymethyl)-1H-imidazol-4-yl]phenoxy}aniline (0.5 g, 1.40 mmol) and ethylisothiocyanate (0.162 g, 1.70 mmol) in 10 ml of ethanol is heated for four hours under reflux. 5 ml of dichloromethane and traces of ethyl acetate and ethanol are added to the residue obtained. The medium is stirred for thirty minutes, then filtered and the solid obtained is dried. A cream-coloured powder is obtained with a yield of 45%.

Provenance & Evidence