Sodium Hydroxide → HCID 44159846, compound

HRID 1930769Notes

Reaction equation

HRID 1930769 reaction equation
C(O)(=O)C(O)=O.[NH2:7][C:8]1[C:13]([C:14]2[O:18][N:17]=[C:16]([CH2:19][OH:20])[CH:15]=2)=[CH:12][CH:11]=[CH:10][N:9]=1.[OH-].[Na+]>O>[NH2:7][C:8]1[C:13]([C:14]2[O:18][N:17]=[C:16]([CH2:19][OH:20])[CH:15]=2)=[CH:12][CH:11]=[CH:10][N:9]=1

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 67355904HCID 67355904, compound

Product 1

HCID 44159846HCID 44159846, compoundYield 67.9%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

To a mixture of [5-(2-aminopyridin-3-yl)isoxazol-3-yl]methanol oxalate (0.39 g) and water (2 mL) was added 5N aqueous sodium hydroxide (0.5 mL) at room temperature and the precipitated solid was filtered to obtain the title compound (0.18 g) as a white solid.

Workup

  1. filtrationthe precipitated solid was filtered

Sources & evidence

ORD record
ord-830586fab9e14b089f74457c4bf1ad33
Source dataset
uspto-grants-2012_05
Patent number
US08188119B2

Reaction notes

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