HuagongsheHuagongshe Chemistry Print Report · For research reference only
tributyl(3,4-dihydro-2H-pyran-6-yl)stannane → 2-Benzyl-5-(5,6-dihydro-4H-pyran-2-yl)-2,3-dihydro-1H-isoindole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tributyl(3,4-dihydro-2H-pyran-6-yl)stannane | HCID 4216837 | — |
| Reactant | 2-Benzyl-5-bromoisoindoline | HCID 53416550 | — |
| Product | 2-Benzyl-5-(5,6-dihydro-4H-pyran-2-yl)-2,3-dihydro-1H-isoindole | HCID 57753659 | — |
Reaction Steps
Prepared in analogy to Example A49(a) from 2-benzyl-5-bromo-2,3-dihydro-1H-isoindole (Example A62(a)) and tributyl-(5,6-dihydro-4H-pyran-2-yl)-stannane. Orange oil. MS (m/e): 292.1 ([M+H]+, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188139B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-2eabdb09ecb0488fa9fa24a957552ce9 |
| Source note | uspto-grants-2012_05 |