Ethanol → 2-Ethoxy-5-methylsulfamoyl-benzoic acid

HRID 1930989Notes

Reaction equation

C[O:2][C:3](=[O:16])[C:4]1[CH:9]=[C:8]([S:10](=[O:14])(=[O:13])[NH:11][CH3:12])[CH:7]=[CH:6][C:5]=1[OH:15].[CH2:17](O)[CH3:18]>>[CH2:17]([O:15][C:5]1[CH:6]=[CH:7][C:8]([S:10](=[O:14])(=[O:13])[NH:11][CH3:12])=[CH:9][C:4]=1[C:3]([OH:2])=[O:16])[CH3:18]

Participants

Reactant 2

HCID 702Ethanol

HCID 230467632-Hydroxy-5-methylsulfamoyl-benzoic acid methyl ester

Product 1

HCID 431452412-Ethoxy-5-methylsulfamoyl-benzoic acid

Procedure

Prepared in analogy to Example B13(d-e) from 2-Hydroxy-5-methylsulfamoyl-benzoic acid methyl ester and ethanol. MS (m/e): 257.9 ([M−H]−, 100%)

Sources & evidence

ORD record: ord-393c27fa0a524dd8abc5d123c34216fc
Source dataset: uspto-grants-2012_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08188139B2

Reaction notes

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