HuagongsheHuagongshe Chemistry Print Report · For research reference only
(+-)-2-Butanol → 2-[(1R)-1-Methylpropoxy]-5-(methylsulfonyl)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (+-)-2-Butanol | HCID 6568 | — |
| Reactant | 2-Fluoro-5-methanesulfonyl-benzoic acid | HCID 22467566 | — |
| Product | 2-[(1R)-1-Methylpropoxy]-5-(methylsulfonyl)benzoic acid | HCID 58863357 | — |
Reaction Steps
Prepared in analogy to Example B4(c) from 2-Fluoro-5-methanesulfonyl-benzoic acid (example B4(b)) and R-(−)-2-butanol. White solid. MS (m/e): 271.1 ([M−H], 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188139B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-d0473b34260544a99303f7e9f2440add |
| Source note | uspto-grants-2012_05 |