Methanol--water (1/1) → HCID 24742426, compound

HRID 1931031Notes

Reaction equation

HRID 1931031 reaction equation
[OH:1][CH:2]([C:20]1[CH:25]=[CH:24][C:23]([O:26][C:27]([F:30])([F:29])[F:28])=[CH:22][CH:21]=1)[CH2:3][CH2:4][C:5]1[CH:17]=[C:16]([CH3:18])[C:8]([O:9][C:10]([CH3:15])([CH3:14])[C:11]([OH:13])=[O:12])=[C:7]([CH3:19])[CH:6]=1.O.[CH3:32]O>>[CH3:32][O:1][CH:2]([C:20]1[CH:25]=[CH:24][C:23]([O:26][C:27]([F:28])([F:29])[F:30])=[CH:22][CH:21]=1)[CH2:3][CH2:4][C:5]1[CH:17]=[C:16]([CH3:18])[C:8]([O:9][C:10]([CH3:15])([CH3:14])[C:11]([OH:13])=[O:12])=[C:7]([CH3:19])[CH:6]=1

Participants

3

Reactant 2

HCID 22242641Methanol--water (1/1)HCID 24742696HCID 24742696, compound

Product 1

HCID 24742426HCID 24742426, compound

Procedure

This compound was prepared following the general procedure E, using a solution of 2-(4-(3-hydroxy-3-(4-(trifluoromethoxy)phenyl)propyl)-2,6-dimethylphenoxy)-2-methylpropanoic acid in a ⅓:⅔ mixture of water/methanol.

Workup

  1. customThis compound was prepared

Sources & evidence

ORD record
ord-20804e479d1c4752a29280622181b0ad
Source dataset
uspto-grants-2012_05
Patent number
US08188148B2

Reaction notes

Loading…