HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Hydroxy-3-(1-phenylmethanesulfonyl-1H-pyrrol-3-yl)-acrylamide → HCID 11348242, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Hydroxy-3-(1-phenylmethanesulfonyl-1H-pyrrol-3-yl)-acrylamide | HCID 73069393 | — |
| Reactant | HCID 86613976 | HCID 86613976 | — |
| Solvent | Methanol--water (1/1) | HCID 22242641 | — |
| Product | HCID 11348242 | HCID 11348242 | — |
Reaction Steps
The method used for preparation of this compound is analogous to the method described for compound 2. Starting materials: (E)-3-[1-(4-dimethylamino-benzene sulfonyl)-1H-pyrrol-3-yl]-N-(tetrahydro-pyran-2-yloxy)-acrylamide (compound A4) (0.200 g), methanol/water 3/2 (50 ml), amberlyst IR15 (0.402 g). Reaction conditions: room temperature, 34 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188138B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-b545ff5f56884dafbc9727a58914970d |
| Source note | uspto-grants-2012_05 |