Acetanilide → HCID 12239330, compound

Participants

Reaction Steps

Method A applied to 4-chloro-3-nitropyridine (79 mg, 0.5 mmol), N-phenylacetamide (81 mg, 0.6 mmol) afforded the title compound as brown solid (76 mg, 73). mp 134-136° C. 1H NMR (DMSO) δ 2.54 (s, 3H), 7.65-7.73 (m, 6H), 8.54 (d, J=5.2Hz, 1H), 9.44 (s, 1H); 13C NMR δ 14.4, 108.2, 126.9, 130.2, 130.3, 133.4, 134.0, 134.8, 139.2, 145.0, 159.2. HRMS (FAB): cal. for C13H12N3 [M+H+]: 210.1031; found: 210.1025.

Provenance & Evidence