Acetanilide → HCID 24821526, compound

Participants

Reaction Steps

Method A applied to 2-chloro-5-methyl-3-nitropyridine (86 mg, 0.5 mmol) and N-phenylacetamide (81 mg, 0.6 mmol) afforded the title compound as brown solid (90 mg, 81%). mp 77-79° C. 1H NMR (DMSO) δ 2.44 (s, 3H), 2.54 (s, 3H), 7.56-7.63 (m, 5H), 7.95 (s, 1H), 8.20 (s, 1H); 13C NMR δ 13.1, 17.9, 124.4, 127.5, 129.5, 129.6, 129.8, 132.9, 145.1, 145.7, 153.2. HRMS (FAB): cal. for C14H14N3 [M+H+]: 224.1187; found: 224.1184.

Provenance & Evidence