Octadecylamine → N-octadecyl-N'-propylsulfamide

HRID 1931790Notes

Reaction equation

[CH2:1]([NH2:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[CH2:20]([NH:23][S:24](Cl)(=[O:26])=[O:25])[CH2:21][CH3:22]>>[CH2:1]([NH:19][S:24]([NH:23][CH2:20][CH2:21][CH3:22])(=[O:26])=[O:25])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]

Participants

Reactant 2

HCID 15793Octadecylamine

HCID 13398949N-propylsulfamoyl chloride

Product 1

HCID 16103197N-octadecyl-N'-propylsulfamideYield 31%

Procedure

The title compound was prepared following the method described in Example 6. The starting reactants are 0.54 g (2.0 mmol) of N-octadecylamine and 0.31 g (2.0 mmol) of N-propylsulfamoyl chloride. 0.06 g of a white solid were obtained. Yield 31%; m.p. 110-112° C.

Sources & evidence

ORD record: ord-a8539e93e2e64d04ae42eef431524246
Source dataset: uspto-grants-2012_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08188312B2

Reaction notes

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