Benzylamine → HCID 2823575, compound

HRID 1932291Notes

Reaction equation

HRID 1932291 reaction equation
Cl[C:2]1[C:7]([N+:8]([O-:10])=[O:9])=[CH:6][CH:5]=[CH:4][N:3]=1.[CH2:11]([NH2:18])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[CH2:11]([NH:18][C:2]1[C:7]([N+:8]([O-:10])=[O:9])=[CH:6][CH:5]=[CH:4][N:3]=1)[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

3

Reactant 2

HCID 7504BenzylamineHCID 796132-Chloro-3-nitropyridine

Product 1

HCID 2823575HCID 2823575, compoundYield 91%

Procedure

In accordance with the same procedures as in Step 1 of Preparation 4, except for using 2-chloro-3-nitropyridine and benzylamine, the titled compound was obtained as yellow solid. (Yield: 91%)

Workup

  1. customIn accordance with the same procedures as in Step 1 of Preparation 4

Sources & evidence

ORD record
ord-c4949ffc95484067aa53bac78511908d
Source dataset
uspto-grants-2012_05
Patent number
US08188114B2

Reaction notes

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