HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethylamine → 1-Methyl-1,2,3,4-tetrahydroisoquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Product | 1-Methyl-1,2,3,4-tetrahydroisoquinoline | HCID 92214 | — |
Reaction Steps
In accordance with the same procedures as in Steps 1, 2, and 3 of Preparation 21, except for using phenethylamine and acetyl chloride, 1-methyl-1,2,3,4-tetrahydroisoquinoline was obtained. In accordance with the same procedures as in Preparation 20, the titled compound was obtained as pale yellow oil. (Yield: 91%) The product was used in the subsequent step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188114B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-343c910ec416436ebb2ad3a46772e92c |
| Source note | uspto-grants-2012_05 |