2,4-Dimethylphenol → 2-(2,4-Dimethylphenoxymethyl)-3-nitropyridine

HRID 1932319노트

반응식

HRID 1932319 반응식
Br[CH2:2][C:3]1[C:8]([N+:9]([O-:11])=[O:10])=[CH:7][CH:6]=[CH:5][N:4]=1.[CH3:12][C:13]1[CH:18]=[C:17]([CH3:19])[CH:16]=[CH:15][C:14]=1[OH:20]>>[CH3:12][C:13]1[CH:18]=[C:17]([CH3:19])[CH:16]=[CH:15][C:14]=1[O:20][CH2:2][C:3]1[C:8]([N+:9]([O-:11])=[O:10])=[CH:7][CH:6]=[CH:5][N:4]=1

참가 물질

3

반응물 2

HCID 77712,4-DimethylphenolHCID 218311782-(Bromomethyl)-3-nitropyridine

생성물 1

HCID 671432272-(2,4-Dimethylphenoxymethyl)-3-nitropyridine수율 78%

실험 절차

In accordance with the same procedures as in Step 3 of Preparation 1, except for using 2-bromomethyl-3-nitropyridine prepared in Step 2 of Preparation 1 and 2,4-dimethylphenol, the titled compound was obtained as yellow solid. (Yield: 78%)

후처리

  1. customIn accordance with the same procedures as in Step 3 of Preparation 1

출처 및 근거

ORD 기록
ord-4dbc08fb75e9411ab3e9576e8601dfdd
출처 데이터셋
uspto-grants-2012_05
특허 번호
US08188114B2

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