HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(1-allyl-2,3-dimethyl-1H-pyrrolo[2,3-c]pyridin-7-ylmethylene)-4-fluorophenylamine → N-[1-(1-allyl-2,3-dimethyl-1H-pyrrolo[2,3-c]pyridin-7-yl)-2-phenylethyl]-4-fluorophenylamine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(1-allyl-2,3-dimethyl-1H-pyrrolo[2,3-c]pyridin-7-ylmethylene)-4-fluorophenylamine | HCID 67141427 | — |
| Reactant | HCID 178418336 | HCID 178418336 | — |
| Product | N-[1-(1-allyl-2,3-dimethyl-1H-pyrrolo[2,3-c]pyridin-7-yl)-2-phenylethyl]-4-fluorophenylamine hydrochloride | HCID 67141466 | 33% |
Reaction Steps
In accordance with the same procedures as in Step 2 of Example 135, except for using N-(1-allyl-2,3-dimethyl-1H-pyrrolo[2,3-c]pyridin-7-ylmethylene)-4-fluorophenylamine prepared in Step 1 of Example 135 and benzylmagnesium chloride, the titled compound was obtained as a white solid. (Yield: 33%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188114B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-c21cb8436066407297cf612b632e134f |
| Source note | uspto-grants-2012_05 |