HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylbenzylamine → 1-(2-methoxyethyl)-2,3-dimethyl-7-(4-methylbenzylamino)-1H-pyrrolo[2,3-c]pyridine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylbenzylamine | HCID 66035 | — |
| Reactant | HCID 11608396 | HCID 11608396 | — |
| Product | 1-(2-methoxyethyl)-2,3-dimethyl-7-(4-methylbenzylamino)-1H-pyrrolo[2,3-c]pyridine hydrochloride | HCID 67142910 | 47% |
Reaction Steps
In accordance with the same procedures as in Step 3 of Example 198, except for using 7-chloro-1-(2-methoxyethyl)-2,3-dimethyl-1H-pyrrolo[2,3-c]pyridine prepared in Step 1 and 4-methylbenzylamine, the titled compound was obtained as a white solid. (Yield: 47%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188114B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-6704dc49a85e410a9b9c2f0ae89259e3 |
| Source note | uspto-grants-2012_05 |