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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1932455Generated: November 3, 2026

Ethanol → HCID 68524463, compound

https://huagongshe.com/reaction/1932455

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthanolHCID 702—
ReactantHCID 68524464HCID 68524464—
CatalystHCID 178503042HCID 178503042—
SolventTetrahydrofuranHCID 8028—
ProductHCID 68524463HCID 68524463—

Reaction Steps

[4-(5-nitropyridin-2-yloxy)phenyl](4-piperonylpiperazin-1-yl)methanone (0.36 g, 0.78 mmol) was dissolved in a mixed solvent consisting of ethanol (5 mL) and THF (5 mL). To the resulting solution was added 5% platinum-carbon (0.06 g), and stirred at room temperature under a hydrogen atmosphere. Two hours later, the 5% platinum-carbon was removed by filtration, and the solvent was evaporated under reduced pressure, to thereby yield 0.32 g of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08188277B2
Source datasetuspto-grants-2012_05
ORD IDord-87814760a24f455eaf20a8ea3d3558ba
Source noteuspto-grants-2012_05