HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 3-(Tribromomethanesulfonyl)benzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-(Tribromomethanesulfonyl)benzoic acid | HCID 22466040 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 3-(Tribromomethanesulfonyl)benzoyl chloride | HCID 22466041 | — |
Reaction Steps
To 3-tribromomethanesulfonylbenzoic acid (B) obtained in the above-described (Step 1) are added dimethylformamide and thionyl chloride and the mixture is refluxed for one hour. The reaction mixture is filtered, and hexane is added to the filtrate to deposit crystals. The crystals are recovered by filtration and dried to obtain 3-tribromomethanesulfonyl benzoylchloride (C) as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06383731B2 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-07448194152749d2a650137d5297eaea |
| Source note | uspto-grants-2002_05 |